This website has a few very nice introductions and activities for flame emission spectroscopy, and outlines a methodology as part of a test prep activity. They're copyrighted, but the underlying methodology seems to be a standard approach, but presented in a clear and concise manner.
http://www.ausetute.com.au/emissions.html
There's also one on atomic absorption (AA) spectroscopy, a variant which may be interesting to us.
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